Lovibond 00386456 - MD1x0/200 - Molybdate HR PP, Molybdate LR PP, Molybdate T Manual do usuário

Tipo
Manual do usuário
Lovibond® Water Testing
Tintometer® Group
Manual of Methods
MD 100 • MD 110 • MD 200
Molybdate
EN
Manual of Methods
Page 4
DE
Methodenhandbuch
Seite 20
ES
Manual de Métodos
Página 36
FR
Méthodes Manuel
Page 52
IT
Manuale dei Metodi
Pagina 68
PT
Métodos Manual
Página 84
NL
Handboek Methoden
Zijde 100
ZH
方法手册
Page 116
NL Handboek van Methoden 01/20EN Handbook of Methods 01/20
KS4.3 T
0.1 - 4 mmol/l KS4.3
Acid / Indicator
20
S:4.3
Instrument specific information
The test can be performed on the following devices. In addition, the required cuvette
and the absorption range of the photometer are indicated.
Instrument Type Cuvette λMeasuring Range
MD 200, MD 600, MD 610,
MD 640, MultiDirect, PM 620,
PM 630
ø 24 mm 610 nm 0.1 - 4 mmol/l KS4.3
SpectroDirect, XD 7000,
XD 7500
ø 24 mm 615 nm 0.1 - 4 mmol/l KS4.3
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
Alka-M-Photometer Tablet / 100 513210BT
Alka-M-Photometer Tablet / 250 513211BT
Application List
Waste Water Treatment
Drinking Water Treatment
Raw Water Treatment
Notes
1. The terms Alkalinity-m, m-Value, total alkalinity and Acid demand to KS4.3 are iden-
tical.
2. For accurate results, exactly 10 ml of water sample must be used for the test.
Display in the MD
100 / MD 110 /
MD 200
Bar code for the
detection of the
methods
Method name
Measuring range
Chemical Method
Method number
Language codes
ISO 639-1 Revision status
KS4.3 T / 20
How to use
ENMethod Reference Book4
EN
Implementation of the provision Acid capacity KS4.3 with Tablet
Select the method on the device
For this method, no ZERO measurements are to be carried out with the following de-
vices: XD 7000, XD 7500
10 ml
Fill 24 mm vial with 10 ml
sample.
Close vial(s).
Sample
Place sample vial in the
sample chamber. • Pay
attention to the positioning.
Dissolve tablet(s) by inver-
ting.
Sample
Place sample vial in the
sample chamber. • Pay
attention to the positioning.
Test
Press the TEST (XD:
START) button.
The result in Acid Capacity KS4.3 appears on the display.
Performing test
procedure
KS4.3 T / 20
NL Handboek van Methoden 01/20EN Handbook of Methods 01/20
How to use
ENMethod Reference Book 5
EN
Molybdate T / M250
ENMethod Reference Book1.06
EN
Molybdate T M250
1 - 50 mg/L MoO4Mo3
Thioglycolate
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
Molybdate HR No. 1 Tablet / 100 513060BT
Molybdate HR No. 1 Tablet / 250 513061BT
Molybdate HR No. 2 Tablet / 100 513070BT
Molybdate HR No. 2 Tablet / 250 513071BT
Set Molybdate No. 1/No. 2 100 Pc.#100 each 517631BT
Set Molybdate No. 1/No. 2 250 Pc.#250 each 517632BT
Remarks
1. The tablets must be added in the correct sequence.
Molybdate T / M250
ENMethod Reference Book1.0 7
EN
Determination of Molybdate HR with Tablet
Select the method on the device.
10 mL
Sample
Fill 24 mm vial with 10 mL
sample.
Close vial(s). Place sample vial in the
sample chamber. Pay
attention to the positioning.
Zero
Press the ZERO button. Remove the vial from the
sample chamber.
Empty vial.
20 mL
Put 20 mL sample in
100 mL measuring beaker
Add MOLYBDATE HR No.
1 tablet .
Crush tablet(s) by rotating
slightly.
Molybdate T / M250
ENMethod Reference Book1.08
EN Add MOLYBDATE HR No.
2 tablet .
Crush tablet(s) by rotating
slightly.
Dissolve the tablets using a
clean stirring rod.
24 mm
Rinse out vial with
prepared sample .
Fill up vial with sample to
the 10 mL mark.
Close vial(s).
Sample
Test
Place sample vial in the
sample chamber. Pay
attention to the positioning.
Press the TEST (XD:
START)button.
The result in mg/L Molybdate/ Molybdenum appears on the display.
Molybdate T / M250
ENMethod Reference Book1.0 9
EN
Analyses
The following table identifies the output values can be converted into other citation
forms.
Unit Cite form Scale Factor
mg/l MoO41
mg/l Mo 0.6
mg/l Na2MoO41.29
Chemical Method
Thioglycolate
Appendix
Interferences
Removeable Interferences
1. Interference from niobium, tantalum, titanium, and zirconium are masked with citric
acid.
2. Interference from vanadium(V) is masked with potassium fluoride.
3. Under test conditions (pH 3.8 – 3.9) iron does not react. Other metals at levels
likely to be found in industrial water systems do not interfere at any significant level
either.
Bibliography
Photometrische Analyse, Lange/ Vjedelek, Verlag Chemie 1980
# including stirring rod, 10 cm
Molybdate LR PP / M251
ENMethod Reference Book1.010
EN
Molybdate LR PP M251
0.03 - 3 mg/L Mo Mo1
Ternary Complex
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
VARIO Molybdenum LR, Set F10 1 Pieces 535450
The following accessories are required.
Accessories Packaging Unit Part Number
Mixing cylinder, 25 ml 1 Pieces 19802650
Preparation
1. Strong alkaline or acidic water samples must be adjusted between pH 3 and pH 5
before the analysis (use 0.5 mol/l Sulphuric acid or 1 mol/l Sodium hydroxide).
2. To avoid errors caused by deposits, rinse the glassware with Hydrochloric acid
(approx. 20%) before the analysis and then rinse with deionised water.
Molybdate LR PP / M251
ENMethod Reference Book1.0 11
EN
Determination of Molybdate LR with Vario Powder Packs
Select the method on the device.
20 mL
Put 20 mL sample in
25 mL measuring cylinder.
Add Vario Molybdenum
1 LR F20 powder pack.
Stopper the mixing cylinder.
Shake to dissolve the
powder.
Blank
24 mm
10 mL
Prepare two clean 24 mm
vials. Mark one as a blank.
Place 10 mL sample in
each vial.
Firmly close the blank .
24 mm
0.5 mL
Place 0.5 mL
Molybdenum 2 LR
solution in the sample
cuvette.
Close vial(s). Invert several times to mix
the contents.
Molybdate LR PP / M251
ENMethod Reference Book1.012
EN
9
4
5
6
7
8
10
11 12
1
2
3
2 min
Blank
Press the ENTER button. Wait for 2 minute(s)
reaction time.
Place blank in the sample
chamber. Pay attention to
the positioning.
Zero
Sample
Press the ZERO button. Remove the vial from the
sample chamber.
Place sample vial in the
sample chamber. Pay
attention to the positioning.
Test
Press the TEST (XD:
START)button.
The result in mg/L Molybdate/ Molybdenum appears on the display.
Molybdate LR PP / M251
ENMethod Reference Book1.0 13
EN
Analyses
The following table identifies the output values can be converted into other citation
forms.
Unit Cite form Scale Factor
mg/l MoO41
mg/l Mo 0.6
mg/l Na2MoO41.29
Chemical Method
Ternary Complex
Appendix
Interferences
Interference from / [mg/L] Influence
Al 50
Cr 1000
Fe 50
Ni 50
NO2 -in all quantities
Cu 10 Leads to higher readings
with a response time of
more than 5 minutes
Bibliography
Analytical Chemistry, 25(9) 1363 (1953)
Molybdate HR PP / M252
ENMethod Reference Book1.014
EN
Molybdate HR PP M252
0.3 - 40 mg/L Mo MO2
Mercaptoacetic Acid
Material
Required material (partly optional):
Reagents Packaging Unit Part Number
VARIO Molybdenum HR, Set F10 1 Set 535300
Preparation
1. Turbid water samples should be passed through a membrane filter prior to analysis.
2. Strongly buffered samples or samples with extreme pH values should, prior
to analysis, be set to a pH of about 7 with 1 mol/l nitric acid or 1 mol/l sodium
hydroxide solution.
Molybdate HR PP / M252
ENMethod Reference Book1.0 15
EN
Determination of Molybdate HR with Vario Powder Packs
Select the method on the device.
10 mL
Sample
Fill 24 mm vial with 10 mL
sample.
Close vial(s). Place sample vial in the
sample chamber. Pay
attention to the positioning.
Zero
Press the ZERO button. Remove the vial from the
sample chamber.
Sample
Add Vario Molybdenum
HR 1 F10 powder pack.
Close vial(s). Swirl around to dissolve the
powder.
Molybdate HR PP / M252
ENMethod Reference Book1.016
EN
Sample
Add Vario Molybdenum
HR 2 F10 powder pack.
Close vial(s). Invert several times to mix
the contents.
Sample
Add Vario Molybdenum
HR 3 F10 powder pack.
Close vial(s). Swirl around to dissolve the
powder.
Sample
Test
9
4
5
6
7
8
10
11 12
1
2
3
5 min
Place sample vial in the
sample chamber. Pay
attention to the positioning.
Press the TEST (XD:
START)button.
Wait for 5 minute(s)
reaction time.
Once the reaction period is finished, the measurement takes place automatically.
The result in mg/L Molybdate/ Molybdenum appears on the display.
Molybdate HR PP / M252
ENMethod Reference Book1.0 17
EN
Analyses
The following table identifies the output values can be converted into other citation
forms.
Unit Cite form Scale Factor
mg/l MoO41
mg/l Mo 0.6
mg/l Na2MoO41.29
Chemical Method
Mercaptoacetic Acid
Appendix
Interferences
Persistant Interferences
1. At concentrations of 10 mg/L Cu, more than the specified 5 minute response time
leads to higher values. A rapid test performance is therefore particularly important.
Interference from / [mg/L]
Al 50
Cr 1000
Fe 50
Ni 50
NO2 -in all quantities
Method Validation
Limit of Detection 0.16 mg/L
Limit of Quantification 0.47 mg/L
End of Measuring Range 40 mg/L
Sensitivity 25.04 mg/L / Abs
Confidence Intervall 0.712 mg/L
Standard Deviation 0.294 mg/L
Variation Coefficient 1.46 %
Molybdate HR PP / M252
ENMethod Reference Book1.018
EN
Bibliography
Analytical Chemistry, 25(9) 1363 (1953)
DE Methodenhandbuch 01/20
KS4.3 T
0,1 - 4 mmol/l KS4.3
Säure / Indikator
20
S:4.3
Instrumentspezifische Informationen
Der Test kann auf den folgenden Geräten durchgeführt werden. Zusätzlich sind die
benötigte Küvette und der Absorptionsbereich der Photometer angegeben.
Geräte Küvette λMessbereich
MD 200, MD 600, MD 610,
MD 640, MultiDirect, PM 620,
PM 630
ø 24 mm 610 nm 0,1 - 4 mmol/l KS4.3
SpectroDirect, XD 7000,
XD 7500
ø 24 mm 615 nm 0,1 - 4 mmol/l KS4.3
Material
Benötigtes Material (zum Teil optional):
Reagenzien Form/Menge Bestell-Nr.
Alka-M-Photometer Tablette / 100 513210BT
Alka-M-Photometer Tablette / 250 513211BT
Anwendungsbereich
Abwasserbehandlung
Trinkwasseraufbereitung
Rohwasserbehandlung
Anmerkungen
1. Die Begrie Alkalität-m, m-Wert, Gesamtalkalität und Säurekapazität KS4.3 sind
identisch.
2. Die exakte Einhaltung des Probevolumens von 10 ml ist für die Genauigkeit des
Analysenergebnisses entscheidend.
Displayanzeige
im MD 100 MD 110
/ MD 200
Barcode zur
Methodenerkennung
Methoden Name
Messbereich
Chemische
Methode
Methodennummer
Sprachkürzel nach
ISO 639-1 Revisionsstand
KS4.3 T / 20
Leitfaden für den Anwender
ENMethod Reference Book20
DE
Durchführung der Bestimmung Säurekapazität KS4.3 mit Tablette
Die Methode im Gerät auswählen.
Für diese Methode muss bei folgenden Geräten keine ZERO-Messung durchgeführt
werden: XD 7000, XD 7500
10 ml
24-mm-Küvette mit 10 ml
Probe füllen.
Küvette(n) verschließen.
Sample
Die Probenküvette in
den Messschacht stellen.
Positionierung beachten.
Tablette(n) durch Um-
schwenken lösen.
Sample
Die Probenküvette in
den Messschacht stellen.
Positionierung beachten.
Test
Taste TEST (XD: START)
drücken.
In der Anzeige erscheint das Ergebnis als Säurekapazität KS4.3.
Durchführung der
Messung
KS4.3 T / 20
DE Methodenhandbuch 01/20
Leitfaden für den Anwender
ENMethod Reference Book 21
DE
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Lovibond 00386456 - MD1x0/200 - Molybdate HR PP, Molybdate LR PP, Molybdate T Manual do usuário

Tipo
Manual do usuário