Lovibond 00386456 - MD1x0/200 - Molybdate HR PP, Molybdate LR PP, Molybdate T Manual do usuário

Lovibond® Water Testing

Tintometer® Group

Manual of Methods

MD 100 • MD 110 • MD 200

Molybdate

EN

Manual of Methods

Page 4

DE

Methodenhandbuch

Seite 20

ES

Manual de Métodos

Página 36

FR

Méthodes Manuel

Page 52

IT

Manuale dei Metodi

Pagina 68

PT

Métodos Manual

Página 84

NL

Handboek Methoden

Zijde 100

ZH

方法手册

Page 116

NL Handboek van Methoden 01/20EN Handbook of Methods 01/20

KS4.3 T

0.1 - 4 mmol/l KS4.3

Acid / Indicator

20

S:4.3

Instrument specific information

The test can be performed on the following devices. In addition, the required cuvette

and the absorption range of the photometer are indicated.

Instrument Type Cuvette λMeasuring Range

MD 200, MD 600, MD 610,

MD 640, MultiDirect, PM 620,

PM 630

ø 24 mm 610 nm 0.1 - 4 mmol/l KS4.3

SpectroDirect, XD 7000,

XD 7500

ø 24 mm 615 nm 0.1 - 4 mmol/l KS4.3

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

Alka-M-Photometer Tablet / 100 513210BT

Alka-M-Photometer Tablet / 250 513211BT

Application List

• Waste Water Treatment

• Drinking Water Treatment

• Raw Water Treatment

Notes

1. The terms Alkalinity-m, m-Value, total alkalinity and Acid demand to KS4.3 are iden-

tical.

2. For accurate results, exactly 10 ml of water sample must be used for the test.

Display in the MD

100 / MD 110 /

MD 200

Bar code for the

detection of the

methods

Method name

Measuring range

Chemical Method

Method number

Language codes

ISO 639-1 Revision status

KS4.3 T / 20

How to use

ENMethod Reference Book4

EN

Implementation of the provision Acid capacity KS4.3 with Tablet

Select the method on the device

For this method, no ZERO measurements are to be carried out with the following de-

vices: XD 7000, XD 7500

10 ml

Fill 24 mm vial with 10 ml

sample.

Close vial(s).

Sample

Place sample vial in the

sample chamber. • Pay

attention to the positioning.

Dissolve tablet(s) by inver-

ting.

Sample

Place sample vial in the

sample chamber. • Pay

attention to the positioning.

Test

Press the TEST (XD:

START) button.

The result in Acid Capacity KS4.3 appears on the display.

Performing test

procedure

KS4.3 T / 20

NL Handboek van Methoden 01/20EN Handbook of Methods 01/20

How to use

ENMethod Reference Book 5

EN

Molybdate T / M250

ENMethod Reference Book1.06

EN

Molybdate T M250

1 - 50 mg/L MoO4Mo3

Thioglycolate

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

Molybdate HR No. 1 Tablet / 100 513060BT

Molybdate HR No. 1 Tablet / 250 513061BT

Molybdate HR No. 2 Tablet / 100 513070BT

Molybdate HR No. 2 Tablet / 250 513071BT

Set Molybdate No. 1/No. 2 100 Pc.#100 each 517631BT

Set Molybdate No. 1/No. 2 250 Pc.#250 each 517632BT

Remarks

1. The tablets must be added in the correct sequence.

Molybdate T / M250

ENMethod Reference Book1.0 7

EN

Determination of Molybdate HR with Tablet

Select the method on the device.

10 mL

Sample

Fill 24 mm vial with 10 mL

sample.

Close vial(s). Place sample vial in the

sample chamber. Pay

attention to the positioning.

Zero

Press the ZERO button. Remove the vial from the

sample chamber.

Empty vial.

20 mL

Put 20 mL sample in

100 mL measuring beaker

Add MOLYBDATE HR No.

1 tablet .

Crush tablet(s) by rotating

slightly.

Molybdate T / M250

ENMethod Reference Book1.08

EN Add MOLYBDATE HR No.

2 tablet .

Crush tablet(s) by rotating

slightly.

Dissolve the tablets using a

clean stirring rod.

24 mm

Rinse out vial with

prepared sample .

Fill up vial with sample to

the 10 mL mark.

Close vial(s).

Sample

Test

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Press the TEST (XD:

START)button.

The result in mg/L Molybdate/ Molybdenum appears on the display.

Molybdate T / M250

ENMethod Reference Book1.0 9

EN

Analyses

The following table identifies the output values can be converted into other citation

forms.

Unit Cite form Scale Factor

mg/l MoO41

mg/l Mo 0.6

mg/l Na2MoO41.29

Chemical Method

Thioglycolate

Appendix

Interferences

Removeable Interferences

1. Interference from niobium, tantalum, titanium, and zirconium are masked with citric

acid.

2. Interference from vanadium(V) is masked with potassium fluoride.

3. Under test conditions (pH 3.8 – 3.9) iron does not react. Other metals at levels

likely to be found in industrial water systems do not interfere at any significant level

either.

Bibliography

Photometrische Analyse, Lange/ Vjedelek, Verlag Chemie 1980

# including stirring rod, 10 cm

Molybdate LR PP / M251

ENMethod Reference Book1.010

EN

Molybdate LR PP M251

0.03 - 3 mg/L Mo Mo1

Ternary Complex

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

VARIO Molybdenum LR, Set F10 1 Pieces 535450

The following accessories are required.

Accessories Packaging Unit Part Number

Mixing cylinder, 25 ml 1 Pieces 19802650

Preparation

1. Strong alkaline or acidic water samples must be adjusted between pH 3 and pH 5

before the analysis (use 0.5 mol/l Sulphuric acid or 1 mol/l Sodium hydroxide).

2. To avoid errors caused by deposits, rinse the glassware with Hydrochloric acid

(approx. 20%) before the analysis and then rinse with deionised water.

Molybdate LR PP / M251

ENMethod Reference Book1.0 11

EN

Determination of Molybdate LR with Vario Powder Packs

Select the method on the device.

20 mL

Put 20 mL sample in

25 mL measuring cylinder.

Add Vario Molybdenum

1 LR F20 powder pack.

Stopper the mixing cylinder.

Shake to dissolve the

powder.

Blank

24 mm

10 mL

Prepare two clean 24 mm

vials. Mark one as a blank.

Place 10 mL sample in

each vial.

Firmly close the blank .

24 mm

0.5 mL

Place 0.5 mL

Molybdenum 2 LR

solution in the sample

cuvette.

Close vial(s). Invert several times to mix

the contents.

Molybdate LR PP / M251

ENMethod Reference Book1.012

EN

9

4

5

6

7

8

10

11 12

1

2

3

2 min

Blank

Press the ENTER button. Wait for 2 minute(s)

reaction time.

Place blank in the sample

chamber. Pay attention to

the positioning.

Zero

Sample

Press the ZERO button. Remove the vial from the

sample chamber.

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Test

Press the TEST (XD:

START)button.

The result in mg/L Molybdate/ Molybdenum appears on the display.

Molybdate LR PP / M251

ENMethod Reference Book1.0 13

EN

Analyses

The following table identifies the output values can be converted into other citation

forms.

Unit Cite form Scale Factor

mg/l MoO41

mg/l Mo 0.6

mg/l Na2MoO41.29

Chemical Method

Ternary Complex

Appendix

Interferences

Interference from / [mg/L] Influence

Al 50

Cr 1000

Fe 50

Ni 50

NO2 -in all quantities

Cu 10 Leads to higher readings

with a response time of

more than 5 minutes

Bibliography

Analytical Chemistry, 25(9) 1363 (1953)

Molybdate HR PP / M252

ENMethod Reference Book1.014

EN

Molybdate HR PP M252

0.3 - 40 mg/L Mo MO2

Mercaptoacetic Acid

Material

Required material (partly optional):

Reagents Packaging Unit Part Number

VARIO Molybdenum HR, Set F10 1 Set 535300

Preparation

1. Turbid water samples should be passed through a membrane filter prior to analysis.

2. Strongly buffered samples or samples with extreme pH values should, prior

to analysis, be set to a pH of about 7 with 1 mol/l nitric acid or 1 mol/l sodium

hydroxide solution.

Molybdate HR PP / M252

ENMethod Reference Book1.0 15

EN

Determination of Molybdate HR with Vario Powder Packs

Select the method on the device.

10 mL

Sample

Fill 24 mm vial with 10 mL

sample.

Close vial(s). Place sample vial in the

sample chamber. Pay

attention to the positioning.

Zero

Press the ZERO button. Remove the vial from the

sample chamber.

Sample

Add Vario Molybdenum

HR 1 F10 powder pack.

Close vial(s). Swirl around to dissolve the

powder.

Molybdate HR PP / M252

ENMethod Reference Book1.016

EN

Sample

Add Vario Molybdenum

HR 2 F10 powder pack.

Close vial(s). Invert several times to mix

the contents.

Sample

Add Vario Molybdenum

HR 3 F10 powder pack.

Close vial(s). Swirl around to dissolve the

powder.

Sample

Test

9

4

5

6

7

8

10

11 12

1

2

3

5 min

Place sample vial in the

sample chamber. Pay

attention to the positioning.

Press the TEST (XD:

START)button.

Wait for 5 minute(s)

reaction time.

Once the reaction period is finished, the measurement takes place automatically.

The result in mg/L Molybdate/ Molybdenum appears on the display.

Molybdate HR PP / M252

ENMethod Reference Book1.0 17

EN

Analyses

The following table identifies the output values can be converted into other citation

forms.

Unit Cite form Scale Factor

mg/l MoO41

mg/l Mo 0.6

mg/l Na2MoO41.29

Chemical Method

Mercaptoacetic Acid

Appendix

Interferences

Persistant Interferences

1. At concentrations of 10 mg/L Cu, more than the specified 5 minute response time

leads to higher values. A rapid test performance is therefore particularly important.

Interference from / [mg/L]

Al 50

Cr 1000

Fe 50

Ni 50

NO2 -in all quantities

Method Validation

Limit of Detection 0.16 mg/L

Limit of Quantification 0.47 mg/L

End of Measuring Range 40 mg/L

Sensitivity 25.04 mg/L / Abs

Confidence Intervall 0.712 mg/L

Standard Deviation 0.294 mg/L

Variation Coefficient 1.46 %

Molybdate HR PP / M252

ENMethod Reference Book1.018

EN

Bibliography

Analytical Chemistry, 25(9) 1363 (1953)

DE Methodenhandbuch 01/20

KS4.3 T

0,1 - 4 mmol/l KS4.3

Säure / Indikator

20

S:4.3

Instrumentspezifische Informationen

Der Test kann auf den folgenden Geräten durchgeführt werden. Zusätzlich sind die

benötigte Küvette und der Absorptionsbereich der Photometer angegeben.

Geräte Küvette λMessbereich

MD 200, MD 600, MD 610,

MD 640, MultiDirect, PM 620,

PM 630

ø 24 mm 610 nm 0,1 - 4 mmol/l KS4.3

SpectroDirect, XD 7000,

XD 7500

ø 24 mm 615 nm 0,1 - 4 mmol/l KS4.3

Material

Benötigtes Material (zum Teil optional):

Reagenzien Form/Menge Bestell-Nr.

Alka-M-Photometer Tablette / 100 513210BT

Alka-M-Photometer Tablette / 250 513211BT

Anwendungsbereich

• Abwasserbehandlung

• Trinkwasseraufbereitung

• Rohwasserbehandlung

Anmerkungen

1. Die Begrie Alkalität-m, m-Wert, Gesamtalkalität und Säurekapazität KS4.3 sind

identisch.

2. Die exakte Einhaltung des Probevolumens von 10 ml ist für die Genauigkeit des

Analysenergebnisses entscheidend.

Displayanzeige

im MD 100 MD 110

/ MD 200

Barcode zur

Methodenerkennung

Methoden Name

Messbereich

Chemische

Methode

Methodennummer

Sprachkürzel nach

ISO 639-1 Revisionsstand

KS4.3 T / 20

Leitfaden für den Anwender

ENMethod Reference Book20

DE

Durchführung der Bestimmung Säurekapazität KS4.3 mit Tablette

Die Methode im Gerät auswählen.

Für diese Methode muss bei folgenden Geräten keine ZERO-Messung durchgeführt

werden: XD 7000, XD 7500

10 ml

24-mm-Küvette mit 10 ml

Probe füllen.

Küvette(n) verschließen.

Sample

Die Probenküvette in

den Messschacht stellen.

Positionierung beachten.

Tablette(n) durch Um-

schwenken lösen.

Sample

Die Probenküvette in

den Messschacht stellen.

Positionierung beachten.

Test

Taste TEST (XD: START)

drücken.

In der Anzeige erscheint das Ergebnis als Säurekapazität KS4.3.

Durchführung der

Messung

KS4.3 T / 20

DE Methodenhandbuch 01/20

Leitfaden für den Anwender

ENMethod Reference Book 21

DE

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Lovibond 00386456 - MD1x0/200 - Molybdate HR PP, Molybdate LR PP, Molybdate T Manual do usuário

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